Dithiophosphoric acids and tetraphosphorus decasulfide in the synthesis ofboron dithiophosphates

Citation
Is. Nizamov et al., Dithiophosphoric acids and tetraphosphorus decasulfide in the synthesis ofboron dithiophosphates, PHOSPHOR SU, 158, 2000, pp. 157-166
Citations number
18
Categorie Soggetti
Inorganic & Nuclear Chemistry
Journal title
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
ISSN journal
10426507 → ACNP
Volume
158
Year of publication
2000
Pages
157 - 166
Database
ISI
SICI code
1042-6507(2000)158:<157:DAATDI>2.0.ZU;2-H
Abstract
The reactions of O,O-dialkyl dithiophosphoric acids with triisobutyl berate , ammonium O,O-diisobutyl dithiophosphate with fluorodiisobutyl berate, and tetraphosphorus decasulfide with triisobutyl berate were studied. On the b asis of these studies, new boron derivatives of dithiophosphoric acids were obtained. Low frequency ultrasonic irradiation (22 kHz, power 130 W) leads to reduction in reaction temperature and time in the reactions studied.