An improved FTIR method for polymer resin beads analysis to support combinatorial solid-phase synthesis

Authors
Liao, JC Beaird, J McCartney, N DuPriest, MT
Citation
Jc. Liao et al., An improved FTIR method for polymer resin beads analysis to support combinatorial solid-phase synthesis, AM LABORAT, 32(14), 2000, pp. 16
Citations number
5
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
AMERICAN LABORATORY
ISSN journal
00447749 → ACNP
Volume
32
Issue
14
Year of publication
2000
Database
ISI
SICI code
0044-7749(200007)32:14<16:AIFMFP>2.0.ZU;2-3
Abstract
When using IR to monitor chemical reactions in solid-phase synthesis, this study shows that the introduction of a thin layer of infrared-transparent K Br to replace the air space between the two diamond windows of a compressio n cell has been found to effectively correct the inconsistent infrared ligh t transmission.