X-ray diffraction techniques using synchrotron radiation play a vital role
in the understanding of structural behavior for a wide range of materials i
mportant in microelectronics, The extremely high flux of X-rays produced by
synchrotron storage rings makes it possible to probe layers and interfaces
in complicated stacked structures, characterize low-atomic-weight material
s such as polymers, and study in situ phase transformations, to name only a
few applications. In this paper, following an introduction to synchrotron
radiation, we describe the capabilities of the IBM/MIT X-ray beamlines at t
he National Synchrotron Light Source (NSLS), Brookhaven National Laboratory
(BNL), A range of techniques are introduced, and examples of their applica
bility to the study of microelectronics-related materials phenomena are des
cribed.