The formation of nano-size ceramic fibers having diameters as small as 20 n
m is described. This material was obtained by a simple precipitation reacti
on from a supercritical aqueous dysprosium bromide solution at high tempera
tures (450 degrees C). The nano-structures have unusually high structural s
tability for extended time periods in this extreme solvent environment. The
experimental procedures are described and analysis of the materials by sca
nning and transition electron microscopy, and x-ray diffraction is presente
d. The new materials may have useful applications as high-strength, corrosi
on resistant materials or as stable catalyst supports for extreme condition
s. (C) 2000 Kluwer Academic Publishers.