T. Kawakatsu et al., Effect of microchannel structure on droplet size during crossflow microchannel emulsification, J SURFACT D, 3(3), 2000, pp. 295-302
A monodispersed oil-in-water emulsion was continuously produced using a cro
ssflow-type silicon microchannel plate in which a liquid flow path for the
continuous phase was made, and on each side of the wall of the path, an arr
ay of regular-sized slits (microchannels) was precisely fabricated on a mic
rometer scale by photolithography. A flat glass plate was tightly attached
to the microchannel plate to cover the top of the microchannels. Regular-si
zed oil (triolein) droplets were generated by pressing the oil through the
microchannels into a continuous phase of 0.3 wt% aqueous sodium lauryl sulf
ate. The average size of the oil droplets was regulated within a range of 1
1.3 to 28.2 mu m by changing the microchannel structural features such as t
he shape of the cross section and outlet, the equivalent diameter, and the
length of the terrace, which is a flat area fabricated at the outlet of the
microchannels. In every case, the droplet size distribution was narrow, an
d the geometric standard deviation was 1.03 or less.