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ENG
TrocCl mediated efficient synthesis of nitriles from primary amides
Authors
Bose, DS
Kumar, KK
Citation
Ds. Bose et Kk. Kumar, TrocCl mediated efficient synthesis of nitriles from primary amides, SYN COMMUN, 30(16), 2000, pp. 3047-3052
Citations number
15
Categorie Soggetti
Organic Chemistry/Polymer Science
Journal title
SYNTHETIC COMMUNICATIONS
ISSN journal
00397911 →
ACNP
Volume
30
Issue
16
Year of publication
2000
Pages
3047 - 3052
Database
ISI
SICI code
0039-7911(2000)30:16<3047:TMESON>2.0.ZU;2-P
Abstract
In order to establish a rapid conversion method of primary amides to nitril es, various types of carboxamides were treated with 2,2,2-trichloroethyl ch loroformate and Et3N, as a dehydrating agent to obtain the desired nitriles in 82-95% yields.