An aged commercial three-way automotive catalyst was examined with res
pect to regeneration procedures. Catalyst samples were leached with ac
etic acid to remove contaminants accumulated on the catalyst surface d
uring operation. The optimum leaching conditions concerning acetic aci
d concentration, solution feed rate and temperature were investigated.
The leached samples were examined for their catalytic activity (CO an
d C2H4 oxidation, NO reduction and N-2 production) in comparison with
samples of fresh and aged catalysts. The leaching procedure improves c
onsiderably the catalytic activity, where in the case of C2H4 oxidatio
n, NO reduction reaches the activity of the fresh catalyst.