The expulsion of interstitial fluid from flocs figures prominently in a wid
e variety of solid-liquid separation processes. particularly wastewater tre
atment and mineral processing. However, our understanding of flee structure
, and particularly of how flocs respond to applied stress, is inadequate fo
r some of the tasks at hand. An experimental technique has been developed i
n which the vertical compression of individual clay-polymer flocs in a cyli
nder-piston apparatus can be observed with macrovideography. The dynamics o
f the compression process have been modeled and the results compared with e
xperiment; the technique has shown an ability to differentiate between floc
structures formed with different polymer dosing regimens. A model of the d
rainage process for interstitial passageways indicates that modest-sized vo
ids drain fairly rapidly relative to the time required for flee compression
. This suggests that expulsion of fluid from passageways during compressive
floc deformation generally occurs sequentially rather than simultaneously.