Synthesis and crystal structure of dibenzyltin dithiopiperidylcarboxylate (PhCH2)(2)Sn(S2CNC5H10)(2)

Authors
Yin, HD Ma, CL Zhang, RF Zhang, LY Dou, JM
Citation
Hd. Yin et al., Synthesis and crystal structure of dibenzyltin dithiopiperidylcarboxylate (PhCH2)(2)Sn(S2CNC5H10)(2), ACH-MODEL C, 137(1), 2000, pp. 103-109
Citations number
16
Categorie Soggetti
Chemistry
Journal title
ACH-MODELS IN CHEMISTRY
ISSN journal
12178969 → ACNP
Volume
137
Issue
1
Year of publication
2000
Pages
103 - 109
Database
ISI
SICI code
1217-8969(2000)137:1<103:SACSOD>2.0.ZU;2-Z
Abstract
The compound (PhCH2)(2)Sn(S2CNC5H10)(2) is prepared by the reaction of dibe nzyltin dichloride with sodium dithiopiperidyl carboxylate. Its crystal str ucture has been determined by X-ray crystallography, it crystallizes in the monoclinic system, space group P2(1)/c with a = 9.71013) Angstrom, b = 24. 36(1) Angstrom, c = 12.393(3) Angstrom, beta = 90.28(2)degrees, V = 293(1) Angstrom(3), and Z = 4.