Major food constituents such as proteins, fats and carbohydrates are genera
lly recognised as having a strong influence on the performance of acid samp
le digestion. Various Scheffe mixture experimental designs were used to det
ect the influence and the interactions between these constituents during th
e Kjeldahl nitrogen digestion using focused microwaves. Pure ingredients we
re mixed in different proportions in order to prepare 7 synthetic food samp
les covering a wide range of foods types. 3 hearing powers were applied and
nitrogen recovery yields were recorded at different times. Two types of mo
dels were proposed to describe the data: one that explains the shape of the
recovery profiles. the other that gives the response surfaces of the recov
ery yield as a function of digestion time. From these models precise guidel
ines to optimise the digestion program of a given food can be deduce.