After more than ten years working with multicomparator instrumental neutron
activation analysis, mainly applied to the characterization of environment
al samples, the Radioisotopes Laboratory (CENA/USP) started changing gradua
lly to the k(0)-method in 1997. The main activities developed, as well as s
ome of the results obtained, are presented here. Even though there is much
more work to be done, the good quality of the results and the possibility o
f elemental determinations without the co-irradiation of standards may lead
to the definitive adoption of the k(0)-method in a near future.