K. Hakala et al., Monitoring of curing process and shelf life of the epoxy-anhydride system with TICT compounds by the fluorescence technique, MACROMOLEC, 33(16), 2000, pp. 5954-5959
In this study the curing degree and the shelf life of an epoxy resin were m
onitored by a fluorescence method, Four extrinsic fluorescence probes, so-c
alled TICT compounds, were used. An intensity ratio method was applied, in
which ratios of the lowest and highest intensity changes in the emission ba
nds are used to determine the degree of the isothermal curing. A smooth and
in some cases a linear correlation was found between the fluorescence inte
nsity ratio and the degree of the cure. The fluorescence technique and the
ratio method enable the monitoring of the precuring and shelf life of the s
tudied epoxy polymer.