An improved procedure is described for the analysis of fibre in samples of
feeding stuffs. The procedure uses a novel cylindrical capsule (FibreCap, p
atent pending) with porous walls having the same filtration characteristics
as Whatman 541 filter paper. The walls are made of hydrophilic material to
facilitate movement of solvents; the Lid is hydrophobic to facilitate gas
exchange. The procedure has been designed to speed up analysis, reduce use
of solvents and reduce variability and systematic error associated with ext
raction and filtration. The FibreCap procedure was compared with convention
al analyses for measurement of crude fibre, neutral and modified acid-deter
gent fibre. Mean values were identical throughout the range of fibre concen
tration found in animal feeding stuffs. However, residual variation was con
sistently lower for FibreCap than for conventional analyses. Two ring tests
were carried out in which results from seven and six collaborating laborat
ories were compared with those at Bristol, Differences between laboratories
were very small although statistically significant. The FibreCap system is
consistent with Statutory Requirements for fibre analysis, more repeatable
than conventional methods and quicker in operation. (C) 2000 Elsevier Scie
nce B.V. All rights reserved.