Synthesis of novel 1-methylindole trimer and tetramer under Friedel-Craftsreaction conditions and determination of their structures by X-ray crystallography
Sb. Mahato et al., Synthesis of novel 1-methylindole trimer and tetramer under Friedel-Craftsreaction conditions and determination of their structures by X-ray crystallography, J CHEM S P1, (16), 2000, pp. 2767-2769
One-step synthesis of novel 1-methylindole trimer and tetramer under Friede
l-Crafts reaction conditions is reported. The use of excess of the substrat
e and the catalyst and application of elevated temperature were necessary f
or success of the synthesis. The complete structures of the products were u
nambiguously elucidated by single-crystal X-ray analysis, and rationalizati
on of their formation is attempted.