A Ti-29 wt % Mg (Ti-45 at % Mg) alloy produced by vapour quenching has
been studied using scanning electron microscopy, transmission electro
n microscopy, energy dispersive X-ray spectroscopy, imaging parallel e
lectron energy-loss spectroscopy and electron diffraction. The alloy i
s shown to be composed of highly supersaturated solid solutions betwee
n two elements hitherto believed to be immiscible. It has a microstruc
ture consisting of columnar units, columnar grains, columnar subgrains
, herring-bone patterns and parallel stripes ranging in size from 15 m
u m to 2 nm. Superimposed on the microstructure are periodic compositi
onal bands with a period of similar to 0.5 mu m. The origins of the pe
riodic compositional bands and the herring-bone patterns are discussed
.