A curing process of epoxy adhesive layers has been investigated by an ultra
sonic pulse spectroscopy and a Brillouin scattering technique. Observed lon
gitudinal elastic wave velocities in the curing layer depended on the veloc
ity in the prepolymer used. From this result, we suggest a simple nondestru
ctive method for the estimation of sample T-g (glass transition temperature
) during cure. The estimated T-g values were in good accordance with the T-
g values easured by differential scanning calorimetry.