Simultaneous determination of beauvericin, enniatins, and fusaproliferin by high performance liquid chromatography

Authors
Monti, SM Fogliano, V Logrieco, A Ferracane, R Ritieni, A
Citation
Sm. Monti et al., Simultaneous determination of beauvericin, enniatins, and fusaproliferin by high performance liquid chromatography, J AGR FOOD, 48(8), 2000, pp. 3317-3320
Citations number
27
Categorie Soggetti
Agricultural Chemistry","Chemistry & Analysis
Journal title
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
ISSN journal
00218561 → ACNP
Volume
48
Issue
8
Year of publication
2000
Pages
3317 - 3320
Database
ISI
SICI code
0021-8561(200008)48:8<3317:SDOBEA>2.0.ZU;2-R
Abstract
A rapid, sensitive and inexpensive HPLC method for routine screening ofbeau vericin, fusaproliferin, and enniatin B-1, A(1), and B has been optimized. Detection limits were determined, ranging between 0.5 and 3.6 ng according to the compound obtained after spiking samples with each mycotoxin at 10-56 mu g/mL concentration range; recoveries averaging from 56 to 74% were obta ined. LC-MS conditions for enniatin analyses by API electrospray technique were set up, this allowing a unique identification of three different ennia tins.