T. Opfermann et al., INVESTIGATION OF ER-IMPLANTED KTIOPO4 CRYSTALS, Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms, 127, 1997, pp. 483-487
KTiOPO4 crystals were implanted with 300 keV Er+ ions at ion fluences
between 1 x 10(13) cm(-2) and 2 x 10(15) cm(-2) and temperatures rangi
ng from 23 degrees C to 750 degrees C, Some of the samples were co-imp
lanted with oxygen at room temperature. The radiation damage as well a
s the Er distribution after implantation and furnace annealing were an
alyzed by means of the RBS-channeling technique. Additionally, photolu
minescence measurements were carried out on some annealed samples. Up
to an implantation temperature T-1 = 200 degrees C amorphous layers ar
e produced already at Er+ ion fluences between N-1 = 1 x 10(13) cm(-2)
and 3 x 10(13) cm(-2). For a dose N-1 = 2 x 10(15) cm(-2) amorphizati
on is prevented for T-1 greater than or equal to 650 degrees C. The re
markable redistribution of Er towards the surface observed after annea
ling at temperatures greater than or equal to 750 degrees C is reduced
by oxygen co-implantation. Complete annealing of amorphous layers in
a K2O atmosphere without any surface decomposition, which normally occ
urs at implantation and annealing temperatures in excess of 650 degree
s C, is found for an annealing temperature of 850 degrees C. After ann
ealing photoluminescence at the wavelength lambda = 1.53 mu m was demo
nstrated in KTiOPO4 for the first time.