Synthesis and characterization of mesoionic 1,3,4-triazolium-2-selenolates

Citation
Pf. De Athayde et al., Synthesis and characterization of mesoionic 1,3,4-triazolium-2-selenolates, PHOSPHOR SU, 161, 2000, pp. 115-121
Citations number
15
Categorie Soggetti
Inorganic & Nuclear Chemistry
Journal title
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
ISSN journal
10426507 → ACNP
Volume
161
Year of publication
2000
Pages
115 - 121
Database
ISI
SICI code
1042-6507(2000)161:<115:SACOM1>2.0.ZU;2-H
Abstract
A new improved synthesis of mesoionic 1,3,4-triazolium-2-selenolates is des cribed and three new members of the series thus obtained. They were charact erized by Elemental Analysis, I.R., H-1 and C-13 NMR and Mass Spectra. The data obtained have been discussed. The chemical shifts at C-2 in the negati ve region and at C-5 in the positive region were compared with data for cor responding mesoionic-2-thiolates. Our data were also compared with availabl e data for some related classes of mesoionic compounds.