Sh. Kang et Jw. Morris, MICROSTRUCTURAL EVOLUTION OF AL-CU THIN-FILM CONDUCTING LINES DURING POST-PATTERN ANNEALING, Journal of applied physics, 82(1), 1997, pp. 196-200
This work reports a statistical analysis of the evolution of polygranu
lar segment lengths during high-temperature annealing of Al(Cu) thin-f
ilm interconnects with quasi-bamboo microstructures. To create samples
of Al(Cu) lines that could be imaged by transmission electron microsc
opy without breaking or thinning, the lines were deposited on electron
-transparent silicon nitride films (the ''silicon nitride window'' tec
hnique). The microstructures of the lines were studied as a function o
f annealing time and temperature. In particular, the distribution of p
olygranular segment lengths was measured. The results show that the lo
nger polygranular segments are preferentially eliminated during post-p
attern annealing. As a consequence, the segment-length distribution na
rrows monotonically during annealing, and changes in shape. The prefer
ential loss of the longest polygranular segments leads to a dramatic i
ncrease in resistance to electromigration failure.