Zero loss peak deconvolution for bandgap EEL spectra

Citation
B. Rafferty et al., Zero loss peak deconvolution for bandgap EEL spectra, J ELEC MICR, 49(4), 2000, pp. 517-524
Citations number
17
Categorie Soggetti
Multidisciplinary
Journal title
JOURNAL OF ELECTRON MICROSCOPY
ISSN journal
00220744 → ACNP
Volume
49
Issue
4
Year of publication
2000
Pages
517 - 524
Database
ISI
SICI code
0022-0744(2000)49:4<517:ZLPDFB>2.0.ZU;2-4
Abstract
This paper shows how bandgap EEL spectra are commonly processed either by d econvolution or subtraction methods in an attempt to remove effects arising from the finite width and long tail of the zero loss peak. This paper will compare the two main methods, and show that the deconvolution method is si gnificantly more reliable and free of user-interpretation or artefacts. We first consider how the zero loss peak is produced and what effects experime ntal conditions have upon it, and then show that only by the deconvolution method can accurate bandgap energies and bandgap densities of states be det ermined.