Double-axis x-ray rocking curve measurements have been used to nondestructi
vely characterize the composition profile of HgCdTe heterojunction photodio
de structures grown by liquid phase epitaxy (LPE). In particular, the thick
ness and composition profile of the thin graded-composition cap layer are d
etermined through an empirical correlation between rocking curve parameters
and composition profiles measured by SIMS. Spatial maps of cap layer thick
ness and composition are generated from automated measurements of x-ray roc
king curves across a wafer. X-ray mapping has been instrumental in improvin
g the spatial uniformity of cap layers and in maintaining control of the gr
owth process in Hg-rich LPE dipping reactors.