Area detector based photon correlation in the regime of short data batches: Data reduction for dynamic x-ray scattering

Citation
D. Lumma et al., Area detector based photon correlation in the regime of short data batches: Data reduction for dynamic x-ray scattering, REV SCI INS, 71(9), 2000, pp. 3274-3289
Citations number
34
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences","Instrumentation & Measurement
Journal title
REVIEW OF SCIENTIFIC INSTRUMENTS
ISSN journal
00346748 → ACNP
Volume
71
Issue
9
Year of publication
2000
Pages
3274 - 3289
Database
ISI
SICI code
0034-6748(200009)71:9<3274:ADBPCI>2.0.ZU;2-2
Abstract
A method for reducing time sequences of raw scattering images to intensity time-autocorrelation functions is presented. The procedure is based on the use of a charge coupled device (CCD) area detector, and optimized for opera ting in the regime of short data batches. Its application to x-ray photon c orrelation spectroscopy (XPCS) measurements is described in detail. Using a slow-scan CCD, we explain how to achieve data acquisition on a 30 ms or fa ster time scale, while simultaneously acquiring data from many coherence ar eas in parallel. The statistical uncertainties of the acquired XPCS data ar e quantified experimentally, and compared to the theoretically expected noi se levels of the correlation functions. (C) 2000 American Institute of Phys ics. [S0034-6748(00)03509-7].