Radiation damping compensation of selective pulses in water-protein exchange spectroscopy

Authors
Cutting, B Chen, JH Moskau, D Bodenhausen, G
Citation
B. Cutting et al., Radiation damping compensation of selective pulses in water-protein exchange spectroscopy, J BIOM NMR, 17(4), 2000, pp. 323-330
Citations number
31
Categorie Soggetti
Biochemistry & Biophysics
Journal title
JOURNAL OF BIOMOLECULAR NMR
ISSN journal
09252738 → ACNP
Volume
17
Issue
4
Year of publication
2000
Pages
323 - 330
Database
ISI
SICI code
0925-2738(200008)17:4<323:RDCOSP>2.0.ZU;2-J
Abstract
The observation of nuclear Overhauser effects (NOEs) between bound water an d biological macromolecules such as proteins and nucleic acids can be impro ved by inverting the water resonance selectively while compensating for rad iation damping effects. The efficiency of inversion, the offset profiles, a nd the appearance of 2D NOE-NOESY spectra can be improved in comparison wit h earlier methods.