Vi. Shapoval et Vv. Malyshev, Electrochemical synthesis of titanium diboride in the dispersed state fromhalide melts, POWD MET ME, 38(11-12), 1999, pp. 556-559
A study is made of the electrolyte deposition of titanium boride powders fr
om halide melts. The conditions required fro the deposition of different ph
ases are determined. On the whole, the synthesis process is controlled by i
nterrelated factors: electrolyte composition, current density, and the temp
erature and duration of the electrolysis operation.