K. Kashihara et al., Nucleation of recrystallized grains in multiple slipped structure without deformation band in aluminum single crystal, MAT SCI E A, 291(1-2), 2000, pp. 207-217
The characteristics of multiple slipped structure and the nucleation of rec
rystallized grains (RGs) have been investigated using pure aluminum single
crystals with an initial tensile axis (TA) orientation of [111] deformed in
tension. By a scanning electron microscope (SEM), very short and wavy slip
traces without deformation bands (DBs) were observed, in which the maximum
misorientation was only approximately 5 degrees. By a transmission electro
n microscope (TEM), it is found that a layered dislocation microstructure c
onsisted of cells with dense dislocation walls (DDWs) was developed. Groups
of the cells were mutually rotated, by approximately 4 degrees, about an a
xis normal to the TA as if they maintained tensile strain and compressive s
train by turns. After annealing, orientations of RGs were mainly rotated at
angles of over 26 degrees about each [111] axis normal to four kinds of [1
11] slip planes in each adjacent deformed matrix (DM). It is renewed in mor
e detail that the nucleation of the RGs with the [111] rotation relationshi
p to each adjacent DM could be explained by the [111] rotation recrystalliz
ation (nucleation) model. The [111] rotation relationships between the defo
rmation textures and the corresponding annealing textures in FCC metals are
selected in both stages of the nucleation of RGs as well as their growth.
(C) 2000 Elsevier Science S.A. All rights reserved.