This work investigates the etching of (110) silicon at 80 degrees C in tetr
a-methyl ammonium hydroxide at 25 wt% and 12 wt%. A wagon-wheel pattern hav
ing spokes spaced 1 degrees apart is used, and the under-etched surfaces an
d inclination angles are observed in detail. Under-etched surfaces are ofte
n complex and composed of two or three facets, some smooth and some rough.
While under-etch rate curves am similar, the inclination angles and crystal
features of the exposed facets vary dramatically between the two concentra
tions.