We have investigated the 2 x 12 degrees symmetric grain boundary of (001) o
riented bicrystalline silicon substrates for high-T-c superconductor applic
ations using scanning focused ion beam (FIB) and electron beam (SEM). We su
ccessfully used the focused ion beam to detect and to mark the grain bounda
ry and hence, to increase the accuracy of positioning the Josephson device
with respect to the grain boundary of the silicon substrate. Both imaging m
ethods have been compared using channeling effects of focused ion and elect
ron beams ill a dual beam system. (C) 2000 Elsevier Science B.V. All rights
reserved.