W. Xue et al., Microstructure and mechanical properties near interface between microarc oxidation coating and Al alloy substrate, SURF ENG, 16(4), 2000, pp. 344-348
The microstructure near the interface between a 2024 Al alloy substrate and
a ceramic coating formed by microarc oxidation has been studied using scan
ning electron microscopy and energy dispersive spectrometry. Hardness and e
lastic modulus on the two sides of the interface were investigated using na
noindentation and Vickers microhardness measurement. The results showed tha
t the microstructure of the substrate was not changed by application of the
coating, and a hardened zone was not observed. During microarc oxidation,
no remelting of the substrate occurred, but remelting of the alumina cerami
c coating on the other side of the interface did take place. The mechanical
properties on the two sines of the interface had obvious differences: in a
certain range of coating thickness there was a gradual increase of hardnes
s and elastic modulus from the interface to the interior of the coating, bu
t hardness remained almost constant in the substrate.