STRUCTURAL INVESTIGATION OF NYLSULFONYL-2-(N-BUTYLSULFONYL)-3,3-DIMETHYLBUTANE

Citation
Vn. Nesterov et al., STRUCTURAL INVESTIGATION OF NYLSULFONYL-2-(N-BUTYLSULFONYL)-3,3-DIMETHYLBUTANE, Crystallography reports, 42(3), 1997, pp. 416-420
Citations number
8
Categorie Soggetti
Crystallography
Journal title
ISSN journal
10637745
Volume
42
Issue
3
Year of publication
1997
Pages
416 - 420
Database
ISI
SICI code
1063-7745(1997)42:3<416:SION>2.0.ZU;2-0
Abstract
The X-ray crystal structure of nylsulfonyl-2-(n-butylsulfonyl)-3,3-dim ethylbutane was determined. The unit-cell parameters are as follows: a = 11.647(4), b = 11.943(4), and c = 13.718(4) Angstrom; alpha = 86.01 (2)degrees, beta = 84.71(2)degrees, and gamma = 77.09(2)degrees; V = 1 850(2) Angstrom(3); d(calc) = 1.244 g/cm(3); Z = 4; and sp. gr. <P(1)o ver bar>. The eclipsed molecular conformation is responsible for the r egio- and stereospecific elimination of the RSO2-group.