Experimental determination of scanning probe microscope cantilever spring constants utilizing a nanoindentation apparatus

Citation
Jd. Holbery et al., Experimental determination of scanning probe microscope cantilever spring constants utilizing a nanoindentation apparatus, REV SCI INS, 71(10), 2000, pp. 3769-3776
Citations number
30
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences","Instrumentation & Measurement
Journal title
REVIEW OF SCIENTIFIC INSTRUMENTS
ISSN journal
00346748 → ACNP
Volume
71
Issue
10
Year of publication
2000
Pages
3769 - 3776
Database
ISI
SICI code
0034-6748(200010)71:10<3769:EDOSPM>2.0.ZU;2-F
Abstract
A rapid, nondestructive, and accurate method for determining the normal spr ing constants of scanning probe microscopy cantilevers is presented. Spring constants are determined using a commercial combination atomic force micro scope and nanoindentation apparatus configured with a W-indenter tip geomet rically configured into either a scanning tunneling microscope pointed tip or chisel shape that may be placed onto the cantilever of interest with hig h accuracy. A load is applied to the cantilever tip and the corresponding d isplacement is measured. From the force-displacement curve, the spring cons tant is determined. For cantilevers with spring constants greater than 1 N/ m, the derived spring constants are believed to be accurate to within +/- 1 0%, with better accuracy for stiffer levers. This method has been used to m easure the stiffness of cantilevers from several manufacturers. (C) 2000 Am erican Institute of Physics. [S0034-6748(00)01010-8].