Jd. Holbery et al., Experimental determination of scanning probe microscope cantilever spring constants utilizing a nanoindentation apparatus, REV SCI INS, 71(10), 2000, pp. 3769-3776
A rapid, nondestructive, and accurate method for determining the normal spr
ing constants of scanning probe microscopy cantilevers is presented. Spring
constants are determined using a commercial combination atomic force micro
scope and nanoindentation apparatus configured with a W-indenter tip geomet
rically configured into either a scanning tunneling microscope pointed tip
or chisel shape that may be placed onto the cantilever of interest with hig
h accuracy. A load is applied to the cantilever tip and the corresponding d
isplacement is measured. From the force-displacement curve, the spring cons
tant is determined. For cantilevers with spring constants greater than 1 N/
m, the derived spring constants are believed to be accurate to within +/- 1
0%, with better accuracy for stiffer levers. This method has been used to m
easure the stiffness of cantilevers from several manufacturers. (C) 2000 Am
erican Institute of Physics. [S0034-6748(00)01010-8].