The microstructure of samples before and after a high current density elect
ropulsing treatment was characterized by using high-resolution transmission
electron microscopy. It has been found that in the coarse-grained Cu-Zn al
loy subjected to the electropulsing treatment, two nanophases were formed,
alpha-Cu(Zn) and beta'-(CuZn), the average grain size of which is about II
nm. A possible mechanism for the formation of nanophases was proposed. The
experimental results indicated that electropulsing, as an instantaneous hig
h-energy input, plays an important role in the nonequilibrium microstructur
al changes in materials and serves as a potential processing approach to sy
nthesize nanostructured materials.