The synthesis and characteristics of SiC nanopowder produced by chemical vapor reaction of SiH4-C2H4-H-2 system

Authors
Citation
Xc. Yang et Zs. Ding, The synthesis and characteristics of SiC nanopowder produced by chemical vapor reaction of SiH4-C2H4-H-2 system, J MATER RES, 15(10), 2000, pp. 2140-2144
Citations number
14
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science","Material Science & Engineering
Journal title
JOURNAL OF MATERIALS RESEARCH
ISSN journal
08842914 → ACNP
Volume
15
Issue
10
Year of publication
2000
Pages
2140 - 2144
Database
ISI
SICI code
0884-2914(200010)15:10<2140:TSACOS>2.0.ZU;2-W
Abstract
SiC nanometer powders were synthesized by the chemical vapor reaction of th e SiH4-C2H4-H-2 system in the temperature range between 1423 K and 1673 K. The effects of processing conditions such as reactive temperature, gas comp osition ratio, and total flow rate on powder characteristics were studied u sing transmission electron microscopy, x-ray diffraction, infrared, Brunaue r-Emmett-Teller, and chemical analyses. A forming mechanism has been propos ed for solid and hollow particles in different processing conditions. The e xperimental results concerning particle growth are discussed according to t he model of G.D. Ulrich er nl., which considers both collision and coalesce nce phenomena.