The crystal structure of K-2[VO(C3H2O4)(2)H2O]center dot 3H(2)O

Authors
Filippova, IG Kiosse, GA
Citation
Ig. Filippova et Ga. Kiosse, The crystal structure of K-2[VO(C3H2O4)(2)H2O]center dot 3H(2)O, RUSS J C CH, 26(9), 2000, pp. 625-628
Citations number
15
Categorie Soggetti
Inorganic & Nuclear Chemistry
Journal title
RUSSIAN JOURNAL OF COORDINATION CHEMISTRY
ISSN journal
10703284 → ACNP
Volume
26
Issue
9
Year of publication
2000
Pages
625 - 628
Database
ISI
SICI code
1070-3284(200009)26:9<625:TCSOKD>2.0.ZU;2-N
Abstract
The crystal structure of a binary malonate, K-2[VO(C3H2O4)(2)H2O]. 3H(2)O, is determined from 3486 unique reflections to R = 0.0496; a = 21.331(8), b = 13.793(7), c = 10.695(4) Angstrom, gamma = 69.16(3)degrees, Z = 8, space group P2(1)/b, rho(calcd) = 1.885(3) g/cm(3). The crystal is composed of th e [VO(C3H2O4)(2)H2O](2-) complex anions, potassium cations, and solvate wat er molecules combined into a three-dimensional framework.