A facile one-pot synthesis of 2,3 '-anhydro-2 '-deoxyuridines via 3 '-O-imidazolylsulfonates

Authors
No, ZS Shin, DS Song, BJ Ahn, M Ha, DC
Citation
Zs. No et al., A facile one-pot synthesis of 2,3 '-anhydro-2 '-deoxyuridines via 3 '-O-imidazolylsulfonates, SYN COMMUN, 30(21), 2000, pp. 3873-3882
Citations number
21
Categorie Soggetti
Organic Chemistry/Polymer Science
Journal title
SYNTHETIC COMMUNICATIONS
ISSN journal
00397911 → ACNP
Volume
30
Issue
21
Year of publication
2000
Pages
3873 - 3882
Database
ISI
SICI code
0039-7911(2000)30:21<3873:AFOSO2>2.0.ZU;2-8
Abstract
Continued interests in the novel synthetic methods of the pivotal compound, 2,3'-anhydro-2'-deoxyribonucleosides (7) uncovered a facile one-pot conver sion of 5 with 1,1'-sulfonyldiimidazole in basic conditions to 7 with almos t quantitative yields (91-99%).