The catalytic activity of complex compounds containing different metal cont
ents immobilized on a silica surface towards the oxidation of carbon monoxi
de and hydrogen has been investigated. In addition, the influence of the co
ncentration of hydrogen and oxygen and the treatment of such catalysts by t
he individual components in the reaction mixture on their catalytic activit
y in the hydrogen oxidation reaction has also been studied. The structural
peculiarities of platinum complexes heterogenized on a silica surface have
been established by diffuse reflectance electronic spectroscopy.