The study of microstructure on a mesoscale by ACOM

Citation
Ra. Schwarzer et A. Huot, The study of microstructure on a mesoscale by ACOM, CRYST RES T, 35(6-7), 2000, pp. 851-862
Citations number
30
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
CRYSTAL RESEARCH AND TECHNOLOGY
ISSN journal
02321300 → ACNP
Volume
35
Issue
6-7
Year of publication
2000
Pages
851 - 862
Database
ISI
SICI code
0232-1300(2000)35:6-7<851:TSOMOA>2.0.ZU;2-X
Abstract
The benefits of analytical electron microscopy are the correlation of morph ology, elemental composition and crystal structure on a submicron scale. Au tomated crystal orientation measurement (ACOM) in the SEM enables, by digit al beam scan, the convenient and fast acquisition of orientation data in se lected bulk surface areas grain by grain. Grain boundaries exceeding some t enth of a degree of misorientation are reliably identified. The quality of backscatter Kikuchi patterns is a (semi-) quantitative measure of local pla stic deformation. The database can be used for crystal orientation mapping (COM), quantitative texture analysis (ODF, pole figures, MODF), characteriz ation of grain and phase boundaries, and orientation stereology in general from macroscopic areas down to mesoscale.