When using sonic nozzles as secondary laboratory standards they must be cal
ibrated. Standard methods of calculating discharge coefficient values are n
ot useful with small nozzles of uncertain geometries. Calibration against p
rimary standards is discussed. Alternatively, one nozzle can be directly co
mpared with another by several techniques using ratios of pressure and temp
erature and sometimes flow. Several factors change the nozzle coefficient.
Estimates of the changes due to pressure and humidity are given. Adiabatic
cooling produces temperature changes that affect the nozzle coefficient by
changing the throat area. Depending on the nozzle holder the inlet gas can
also be cooled with an effect on the flow. Nozzles may be made by metal mac
hining or by shrinking glass tubes. Sapphire cutting heads, which may be bo
ught, can be used as sonic nozzles. An example of a promising but unsuitabl
e form of nozzle having a square throat is given. The pressure dependence o
f these is discussed. The use of nozzles in arrays, for automatic operation
as flow standards, is described. (C) 2000 Elsevier Science Ltd. All rights
reserved.