The Kiel/Berlin pressure cells for neutron powder diffraction

Citation
K. Knorr et W. Depmeier, The Kiel/Berlin pressure cells for neutron powder diffraction, HIGH PR RES, 17(3-6), 2000, pp. 297-303
Citations number
8
Categorie Soggetti
Physics
Journal title
HIGH PRESSURE RESEARCH
ISSN journal
08957959 → ACNP
Volume
17
Issue
3-6
Year of publication
2000
Pages
297 - 303
Database
ISI
SICI code
0895-7959(2000)17:3-6<297:TKPCFN>2.0.ZU;2-8
Abstract
Two piston/cylinder type pressure cells for neutron powder diffraction are presented. They provide a large sample volume and hence allow rapid data co llection at moderate flux neutron sources. Structure refinements from the d iffraction data are possible. The maximum attainable pressure is above 2 GP a for Ti/Zr zero-scattering pressure cylinders. Both cells may be equipped with a micro-furnace. This allows measurement up to 700 K, simultaneously t o the application of pressure. The low temperature setup for the cell-I is presented which will allow experiments down to 1.5 K.