J. Lee et Af. Yee, Inorganic particle toughening I: micro-mechanical deformations in the fracture of glass bead filled epoxies, POLYMER, 42(2), 2001, pp. 577-588
General characteristics of micro-mechanical deformations found in the fract
ure of various glass bead filled epoxies are investigated. Among the variou
s types of step features on fracture surfaces, the basic longitudinal textu
re is not influenced by the existence of glass beads, but most other steps
formed are significantly affected. Various microscopic investigations show
that microcracking does not extensively occur in the fracture of glass bead
filled epoxies. Microcracking other than debonding of glass beads is seldo
m observed, and furthermore, debonding is found to occur only on and near t
he fracture surface. Micro-shear bands are clearly identified and distingui
shed from microcracks found in unnotched tensile specimens. Based on examin
ation of micro-mechanical deformations, three types of fracture processes a
re proposed for glass bead filled epoxies having different glass bead conte
nts and interfacial strengths. (C) 2000 Elsevier Science Ltd. All rights re
served.