A. Boutillon et al., Indirect measurement of the alcohol concentration during the industrial distillation of Cognac., SCI ALIMENT, 20(3), 2000, pp. 347-365
Distillate alcohol concentration is an important parameter in the two step
distillation used to produce Cognac spirit. Consequently on line measuremen
t of alcohol concentration is useful. Nevertheless the sensors currently ma
rketed are not suitable, due to their lack of precision, their cost or due
to volume implementation constraints. This paper reports the development or
an indirect measure for industrial applications. It is based on the measur
ement of two parameters 1) the temperature of the saturated distillate stea
m, 2) the atmospheric pressure and also on a model relating these Values to
the alcohol concentration. Two models were proposed which allowed high pre
cision over the whole range of alcohol concentrations (0-80% vol.): A polyn
omial model gave a good accuracy for high concentrations (from 80 to 60% vo
l.) corresponding to the extraction of the "heart", whilst a recurrent neur
al network was necessary for the lower range (from 60 to 2% vol.). The aver
age accuracy of the measures was +/- 0.7% vol.; The method was sucessfully
tested on stills of Various sizes (25 hL and 100 hL), thus demonstrating th
at is can be easily implemented in other industrial applications. The indir
ect evaluation of alcohol concentration reported herein, which was tested o
n two industrial stills, is now being routinely used for industrial distill
ation.