Hemisynthesis of bistramide D by stereoselective reduction of bistramide A. Partial determination of relative and absolute configurations

Citation
G. Solladie et al., Hemisynthesis of bistramide D by stereoselective reduction of bistramide A. Partial determination of relative and absolute configurations, TETRAHEDR L, 41(40), 2000, pp. 7747-7750
Citations number
14
Categorie Soggetti
Chemistry & Analysis","Organic Chemistry/Polymer Science
Journal title
TETRAHEDRON LETTERS
ISSN journal
00404039 → ACNP
Volume
41
Issue
40
Year of publication
2000
Pages
7747 - 7750
Database
ISI
SICI code
0040-4039(20000930)41:40<7747:HOBDBS>2.0.ZU;2-W
Abstract
The hemisynthesis of bistramide D by stereoselective reduction of bistramid e A is reported. The absolute configuration of C4 in bistramide D was also determined and the relative configurations of C6, C9 and C11 in the pyran p art, as well as those of C22, C23, C27 and C31 in the spiro moiety of bistr amides A and D were also determined by NMR. (C) 2000 Published by Elsevier Science Ltd.