Crystal structure of Tutton's salts, Rb-2[M-II(H2O)(6)] (SO4)(2), M-II = Mg, Mn, Fe, Co, Ni, Zn

Citation
H. Euler et al., Crystal structure of Tutton's salts, Rb-2[M-II(H2O)(6)] (SO4)(2), M-II = Mg, Mn, Fe, Co, Ni, Zn, Z KRIST-NEW, 215(4), 2000, pp. 473-476
Citations number
5
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES
ISSN journal
14337266 → ACNP
Volume
215
Issue
4
Year of publication
2000
Pages
473 - 476
Database
ISI
SICI code
1433-7266(2000)215:4<473:CSOTSR>2.0.ZU;2-H
Abstract
H12MgO14Rb2S2, monoclinic, P12(1)/a1 (No. 14), a = 9.226(2) Angstrom, b = 1 2.472(2) Angstrom, c = 6.217(2) Angstrom, beta = 105.98(1)degrees, V = 687. 7 Angstrom(3), Z = 2, R-gt(F) = 0.022, wR(all)(F-2) = 0.049, T = 293 K. H12MnO14Rb2S2, monoclinic, P12(1)/a1 (No. 14), a = 9.282(2) Angstrom, b = 1 2.600(2) Angstrom, c = 6.254(2) Angstrom, beta = 105.94(2)degrees, V = 703. 3 Angstrom(3), Z = 2, R-gt(F) = 0.018, wR(all)(F-2) = 0.039, T = 293 K. FeH12O14Rb2S2, monoclinic, P12(1)/a1 (No. 14), a = 9.224(2) Angstrom, b = 1 2.510(3) Angstrom, c = 6.255(1) Angstrom, beta = 105.75(2)degrees, V = 694. 7 Angstrom(3), Z = 2, R-gt(F) = 0.022, wR(all)(F-2) = 0.050, T = 293 K. CoH12O14Rb2S2, monoclinic, P12(1)/a1 (No. 14), a = 9.197(2) Angstrom, b = 1 2.446(2) Angstrom, c = 6.236(1) Angstrom, beta = 106.04(1)degrees, V = 686. 1 Angstrom(3), Z = 2, R-gt(F) = 0.018, wR(all)(F-2) = 0.039, T = 293 K. H12NiO14Rb2S2, monoclinic, P12(1)/a1 (No. 14), a = 9.131(2) Angstrom, b = 1 2.410(2) Angstrom, c = 6.221(2) Angstrom, beta = 106.06(2)degrees, V = 677. 5 Angstrom(3), Z = 2, R-gt(F) = 0.017, wR(all)(F-2) = 0.042, T = 293 K. H12O14Rb2S2Zn, monoclinic, P12(1)/a1 (No. 14), a = 9.179(3) Angstrom, b = 1 2.441(4) Angstrom, c = 6.239(2) Angstrom, beta = 105.93(3)degrees, V = 685. 1 Angstrom(3), Z = 2, R-gt(F) = 0.018, wR(all)(F-2) = 0.041, T = 293 K.