Crystal structure of (1R,2R,4S,6R,8S)-2 ',2 '-dimethoxy-8-hydroxy-spiro[3,5,10-trioxa-tricyclo[6.2.1.0(2,6)]undecan-4,1 '-cyclohexan]-9-one monohydrate, C15H24O8 and of (1R,2R,4R,6R,8S)-2 ',2 '-dimethoxy-8-hydroxyspiro[3,5,10-trioxatricyclo[6.2.1.0(2'6)]undecan-4,1 '-cyclohexan]-9-one, C15H22O7

Authors
Kelling, A Schilde, U Sefkow, M
Citation
A. Kelling et al., Crystal structure of (1R,2R,4S,6R,8S)-2 ',2 '-dimethoxy-8-hydroxy-spiro[3,5,10-trioxa-tricyclo[6.2.1.0(2,6)]undecan-4,1 '-cyclohexan]-9-one monohydrate, C15H24O8 and of (1R,2R,4R,6R,8S)-2 ',2 '-dimethoxy-8-hydroxyspiro[3,5,10-trioxatricyclo[6.2.1.0(2'6)]undecan-4,1 '-cyclohexan]-9-one, C15H22O7, Z KRIST-NEW, 215(4), 2000, pp. 515-518
Citations number
3
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES
ISSN journal
14337266 → ACNP
Volume
215
Issue
4
Year of publication
2000
Pages
515 - 518
Database
ISI
SICI code
1433-7266(2000)215:4<515:CSO(''>2.0.ZU;2-9
Abstract
C15H24O8, monoclinic, P12(1)1 (No. 4), a = 6.581(2) Angstrom, b = 7.373(2) Angstrom, c = 16.681(3) Angstrom, beta = 91.10(2)degrees, V = 809.1 Angstro m(3), Z = 2, R-gt(F) = 0.036, w(Ref)(F-2)= 0.111, T = 298 K. C15H22O7. mono clinic, P12(1)1 (No. 4), a = 12.2868(8) Angstrom, b = 8.2168(5) Angstrom, c = 14.8921(9) Angstrom, beta = 98.571(5)degrees V = 1486.7 Angstrom(3), Z = 4 R-gt(F) = 0.037, wR(ref)(F-2) = 0.115, T = 298 K.