Polymorphism in 4-methyl-1,2,4-triazolethione

Authors
Elhajji, A Zaydoun, S Benarafa, L Idrissi, MS Lautie, A Romain, F
Citation
A. Elhajji et al., Polymorphism in 4-methyl-1,2,4-triazolethione, J RAMAN SP, 31(10), 2000, pp. 951-953
Citations number
12
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
JOURNAL OF RAMAN SPECTROSCOPY
ISSN journal
03770486 → ACNP
Volume
31
Issue
10
Year of publication
2000
Pages
951 - 953
Database
ISI
SICI code
0377-0486(200010)31:10<951:PI4>2.0.ZU;2-L
Abstract
Raman and infrared spectra of 4-methyl-1,2,4-triazolethione showed that two crystalline phases, one stable and the other metastable, can be obtained f rom various crystallization processes. The metastable phase transforms into the stable phase at 395 K by an irreversible first-order phase transition. The two phases were characterized spectroscopically and structural propert ies are discussed. Copyright (C) 2000 John Whey & Sons, Ltd.