A procedure of yttrium and strontium separation from calcium and other cati
ons has been developed for rapid determination of Sr-90 in soil samples. Th
e procedure involves yttrium, strontium and other cations bound on cation e
xchanger AMBERLITE IR-120, separtion of yttrium and strontium from other ca
tions, e.g, potassium, calcium, sodium, barium, on anion exchangers AMBERLI
TE CG-400 or DOWEX AG Ix 8 with 0.25 mol l(-1) HNO3 in alcohol mixture as e
luent, separation of yttrium from strontium on cation exchanger DOWEX 50 x
8 with 3 mol l(-1) HNO3, and determination of Sr-90 on the low-level gas-fl
ow beta -counter and by Cherenkow counting on the liquid-scintillation coun
ter. It has been shown that this procedure might be successfully applied in
rapid determination of Sr-90, in a timesaving manner and without applicati
on of strong, concentrated acids. The method is appropriate for determinati
on of the water soluble fraction of Sr-90 in different kinds of environment
al samples (milk, water, wine, vegetables, etc.) with some modification of
the sample preparation procedure.