Citation
Ta. Khan et al., Synthesis and characterization of 13,14-membered tetraazamacrocyclic complexes, I J CHEM A, 39(4), 2000, pp. 450-452
Citations number
24
Categorie Soggetti
Chemistry
Journal title
INDIAN JOURNAL OF CHEMISTRY SECTION A-INORGANIC BIO-INORGANIC PHYSICAL THEORETICAL & ANALYTICAL CHEMISTRY
ISSN journal
03764710
→ ACNP
Volume
39
Issue
4
Year of publication
2000
Pages
450 - 452
Database
ISI
SICI code
0376-4710(200004)39:4<450:SACO1T>2.0.ZU;2-K
Abstract
Oxotetraazamacrocyclic transition metal complexes, [(MLCl2)-Cl-1] or [(MLCl
2)-Cl-2] [M = Co-II, Ni-II, Cu-II and Zn-II] have been synthesized by the t
emplate condensation reaction of o-aminobenzoic acid, diethylenetriamine an
d 1,3-dibromopropane or dibromoethane in methanol medium. All the complexes
have been characterized on the basis of elemental analysis, IR, H-1 NMR, E
PR, UV-vis, conductivity and magnetic moment data. All the complexes are no
n-ionic in nature and exhibit an octahedral geometry.