Comparative study of continuous-power and pulsed-power microwave curing ofepoxy resins

Authors
Citation
B. Fu et Mc. Hawley, Comparative study of continuous-power and pulsed-power microwave curing ofepoxy resins, POLYM ENG S, 40(10), 2000, pp. 2133-2143
Citations number
20
Categorie Soggetti
Material Science & Engineering
Journal title
POLYMER ENGINEERING AND SCIENCE
ISSN journal
00323888 → ACNP
Volume
40
Issue
10
Year of publication
2000
Pages
2133 - 2143
Database
ISI
SICI code
0032-3888(200010)40:10<2133:CSOCAP>2.0.ZU;2-P
Abstract
Three epoxy reaction systems, diglycidyl ether of bisphenol A (DGEBA) with curing agents meta phenylene diamine (mPDA), diaminodliphenyl methane (DDM) , and diaminodiphenyl sulfone (DDS), were cured with both pulsed-power and continuous-power microwave curing systems. Isothermal curing was conducted at three different temperatures for each reaction system with both pulsed-p ower and continuous-power microwave curing systems. Extent of cure was meas ured with Fourier Transform Infrared Spectroscopy (FTIR). The temperature c haracteristics, incident and reflected power patterns, and the reaction rat es were compared between the two curing approaches. The incident power and reflected power of both curing processes were observed to reveal reaction s tatus. Continuous-power microwave curing produced noticeably higher reactio n rates than pulsed-power microwave curing.