Xy. Li et Kn. Tandon, Microstructural characterization of mechanically mixed layer and wear debris in sliding wear of an Al alloy and an Al based composite, WEAR, 245(1-2), 2000, pp. 148-161
The present work was undertaken to characterize mechanically mixed layers (
MML) and wear debris formed during sliding wear of an AI-Si alloy and an AI
-Si/SiCp metal matrix composite against M2 tool steel under dry sliding con
ditions. In particular, chemical, microstructural and crystallographic char
acteristics of the MMLs and wear debris have been investigated using scanni
ng electron microscopy (SEM), transmission electron microscopy (TEM) with e
nergy dispersive spectroscopy (EDS) and X-ray diffraction (XRD), as well as
Mossbauer spectroscopy. It was observed that MMLs were formed in the worn
surfaces at a variety of sliding loads used in the present work. The result
s show that the mixed layers and wear debris generated from the sliding sys
tems had similar microstructural features and were comprised of a mixture o
f ultrafine grained structures, in which the constituents varied depending
on the sliding loads. At a low load, the ultrafine structures mainly consis
ted of the original base materials, i.e. alpha -AI solid solution and alpha
-Fe from the steel. With an increase in sliding load, the ultrafine struct
ures were incorporated with an Fe-AI(Si) intermetallic compound and an alum
inum oxide. The formation mechanisms of the mechanically mixed layers and t
heir influences on wear mechanisms of these multiphase materials were also
studied on the basis of the microstructural observations. (C) 2000 Publishe
d by Elsevier Science S.A.