A series of new s-triazolo[3, 4-b]-1, 3, 4-thiadiazole, 1, 2, 4-triazole an
d 1, 3, 4-oxadiazole derivatives were synthesized from 6-nitrobenzimidazol-
1-acetic acid hydrazide and 4-amino-5-mercapto-3(6-nitrobenzimidazol-1-meth
ylene)-1, 2, 4-triazole, respectively. The structures of the compounds synt
hesized were confirmed by elemental analyses, H-1 NMR, IR and MS. Their spe
ctral properties were also discussed.